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Beilstein J. Org. Chem. 2013, 9, 2886–2897, doi:10.3762/bjoc.9.325
Graphical Abstract
Scheme 1: General Heck reaction showing the possible isomers that can be produced.
Figure 1: Schematic diagram of the stirred autoclave reactor. Pickel’s pump NWA PM101 was used to achieve sup...
Figure 2: Schematic diagram of the continuous flow system. The reactor shown is the 3.9 mm i.d. PFR. For the ...
Figure 3: Total conversion of 4-iodoanisole as a function of reactor run time for three reaction temperatures....
Figure 4: Total conversion of 4-iodoanisole at 155 °C and 200 bar as a function of reactor run time for diffe...
Figure 5: Total conversion of 4-iodoanisole as a function of reactor run time at 145 °C and at 200 (●) and 25...
Figure 6: Conversion of 4-iodoanisole to methyl 4-methoxycinnamate (●) at 155 °C and 200 bar as a function of...
Figure 7: Comparison of conversion as a function of reactor run time for the reaction of methyl acrylate in t...
Figure 8: TOF values for the 1 mm (ο) and 3.9 mm (●) PFRs at a total flow rate of 0.12 mL min−1, 155 °C and 2...
Figure 9: Turnover frequencies of the Heck reactions at 155 °C using styrene (ο) as combined isomeric product...